Synthesis of 10.
- Vignir Isberg (481361)
- James Paine (481362)
- Sebastian Leth-Petersen (481363)
- Jesper L. Kristensen (141358)
- David E. Gloriam (481364)
Publication date
November 2013
DOIAbstract
<p>Reagents and Conditions: (a) NaBH<sub>4</sub>, EtOH, r.t., 2 h; (b) Me<sub>3</sub>SiCN, BF<sub>3</sub>.Et<sub>2</sub>O, CH<sub>2</sub>Cl<sub>2</sub>, −78°C to r.t.; (c) DIBALH, THF, reflux, 2 h. The 7-bromochroman-4-one 16 was prepared as previously described.<a href="http://www.plosone.org/article/info:doi/10.1371/journal.pone.0078515#pone.0078515-Selander1" target="_blank">[23]</a></p
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