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A physicochemical survey of water quality and benthic macroinvertebrates at two rivers namely Sungai Dekong and Dawai in Lojing Highland was conducted on 23 and 24, January 2014. Three stations were selected for physicochemical water quality, one station at Sungai Dekong and two other stations at Sungai Dawai. On the other hand, benthic macroinvertebrates were collected at nine stations, i.e. three stations at Sungai Dekong and the other six stations at Sungai Dawai. Result shows that, Station 1 (Sungai Dekong) recorded Very Poor Biological Monitoring Working Party, BMW