In this paper we present a method for the measurement of mass fractions of iron ore in two-phase flows consisting of water and iron ore particles. The proposed method uses a clamp-on PVDF transmitter and a 12-element PVDF receiver array to measure the excess attenuation of pulsed ultrasound due to the presence of particles. From the measured data we are able to extract a quantity that varies linearly with particle mass fraction in the range from 0 to 13%. With the proposed method we can measure the mass fraction in whole percent, at a 95% confidence level. Using an array of receivers we are also able to calculate an attenuation profile over a cross section of the flow, which indicates how the particles are distributed within the flow. This ...