The use of a paratellurite acousto-optic tunable ® lter (AOTF) is demonstrated as a monochromator for spectrophotometry. This device operates in the range of 400 to 700 nm with a resolution from 2.5 nm (at 633 nm) to 0.5 nm (at 400 nm). Results of the initial characterizations indicate that behavior follows the theoretical model in terms of frequency/wavelength relationships, dependence of the output wavelength upon the incident radiation angle, and bandpass as a function of wavelength. Initial results of spectroscopic characterizations of permanganate, cobalt(II), holmium(III), praseodymium( III), and neodymium(III) solutions are presented. Placing a polarizer in the light path reduced the amount of stray light reaching the dete...