Evaluation of Creep Property of AS800 Silicon Nitride from As-Processed Surface Regions

Tensile creep studies were carried out to evaluate the creep performance of AS800 silicon nitride samples extracted from the surface and bulk regions of as-processed billets at 1350 C in air. The objective of this study was to understand the creep properties of the silicon nitride in the as-processed surface region and determine if they are comparable to those obtained from the bulk region. The results indicated that samples from the as-processed surface region exhibited higher creep rates and shorter lifetimes as compared with those obtained from the bulk region. The poor creep performance of material from the as-processed surface region was due to the higher content of glassy phase enriched with oxygen and sintering additive elements