Structure of (1α,3β,5α)-5-chloro-1,3-diphenyl-5-bis(trimethylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-dithiatriazaphosphorine 1,3-dioxide

Meetsma, A.
Herrema, J. K.
van de Grampel, J. C.

Publication date

January 1988

DOI

Abstract

C19H29CIN302PS2Si~, Mr=518"17, monoclinic, P21/n, a= 10.751 (3), b= 22.48 (1), c= 10.942 (3)A, fl=108.58(2) ° , V=2507(2)A 3, Z= 4, D x= 1.373gcm -3, MoK~, 2=0.71073A, g= 4.9 cm -x, F(000) = 1088, T= 130 K, R = 0.069 for 2831 observed reflections with I> 2.5a(I). The inorganic ring skeleton has an envelope conformation. The S-N and P-N bond lengths (mean values) are 1.562 (6) and 1.590 (8)A, respectively. One of the phenyl rings exhibits a disordered behaviour

Extracted data

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Structure of (1α,3β,5α)-5-chloro-1,3-diphenyl-5-bis(trimethylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-dithiatriazaphosphorine 1,3-dioxide

Abstract

Extracted data

Structure of (1α,3β,5α)-5-chloro-1,3-diphenyl-5-bis(trimethylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-dithiatriazaphosphorine 1,3-dioxide

Abstract

Extracted data

Related items

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Structure of (1α,3β,5α)-5-chloro-1,3-di­phenyl-5-bis­(tri­methylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-di­thiatri­aza­phosphorine 1,3-dioxide

Abstract

Extracted data

Structure of (1α,3β,5α)-5-chloro-1,3-di­phenyl-5-bis­(tri­methylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-di­thiatri­aza­phosphorine 1,3-dioxide

Abstract

Extracted data

Related items

Related items

Structure of (1α,3β,5α)-5-chloro-1,3-diphenyl-5-bis(trimethylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-dithiatriazaphosphorine 1,3-dioxide

Structure of (1α,3β,5α)-5-chloro-1,3-diphenyl-5-bis(trimethylsilyl)methyl-1λ6,3λ6,2,4,6,5λ5-dithiatriazaphosphorine 1,3-dioxide