Intercomparison exercise on difficult to measure radionuclides in spent ion exchange resin

A need for method validation in radiochemical analyses of decommissioning waste is a challenging task due to lack of commercial reference materials. Participation in an intercomparison exercise is one way for a laboratory to assess their performance and validate their analysis results. A three-year project within the Nordic Nuclear Safety Research (NKS) community was initiated in order to carry out intercomparison exercises on difficult to measure (DTM) radionuclides in real decommissioning waste. Both Nordic and Non-Nordic laboratories participated. This paper reports the results from the final year of the project focusing on beta- and gamma emitter (i.e., easy to measure, ETM) analysis in spent ion exchange resin. The assigned values were derived from the participants’ results according to ISO 13528 standard and the performances were assessed using z scores. The results showed generally good performances for both DTMs and ETMs