Crystal structure of (cyclohexanonetriphenylphosphonium)(trichlorotriphenyl)palladate(II)-benzene(1/1), [(C6H5)3P(CHCH2CO(CH2)3)][C6H5)3PPdCl3].C6H6
- U. CASELLATO
- R. GRAZIANI
- L. TONIOLO
- CAVINATO, GIANNI
Publication date
January 2000
DOI Publisher
R Oldenbourg Verlag:Rosenheimerstrasse 145, D 81671 Munich Germany:011 49 89 45051229, INTERNET: http://www.oldenbourg.de, Fax: 011 49 89 45051207 ISSN
2197-4578Abstract
Synthesis and crystal structure of (cyclohexanonetriphenylphosphonium)(trichlorotriphenyl)palladate(II)-benzene(1/1), [(C6H5)3P(CHCH2CO(CH2)3)][C6H5)3PPdCl3].C6H6. C48H45Cl3P2Pd, triclinic, P1 (No.2), a = 9.225(4) Å, b = 13.734(5) Å, c = 18.056(6) Å, alfa=74.48(3)°, beta = 94.40(3)°, gamma= 98.82(3)°, V = 2176.6 Å3, Z =2, R(F )= 0.084, T = 293K
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