The paper describes the application of the azimuthal scan technique for absolute structure determination using X-ray anomalous dispersion. A diffraction pattern with rotation around the scattering vector provides information about various anisotropic effects: absorption, extinction and multi-beam interaction. Recording of azimuthal scans for Friedel pairs is proposed as an alternative to single reflection measurement. Several factors affecting the smoothness of the azimuthal scan curves are discussed and a procedure for eliminating various sources of errors, involving a Fourier filtering, is proposed in order to increase feasibility of chiral discrimination
International audienceThe calibration of high-energy X-ray diffraction setups using an area detector...
Owing to the two-dimensional periodicity of a superstructure on the crystal surface, the intensity i...
This tutorial review article discusses chirality determination in the solid state, both in single cr...
The paper discusses several feasibility prediction criteria with particular emphasis on light atom m...
Single-crystal X-ray crystallography is the major analytical technique in use today for absolute-con...
Abstract. The first step in solving macromolecular crys-tal structures by multi- or single-wavelengt...
The paper describes measuring methods of weak resonant scattering signals occurring in X-ray diffrac...
It is shown that three-beam X-ray diffraction provides a means of resolving the enantiomorphism prob...
The phases of X-ray reflection of a crystal can be measured, except for an ambiguity, if the crystal...
Fundamental notions concerning absolute structure and absolute configuration, and their determinatio...
A Fortran program has been developed for the reduction of single-crystal diffraction data from a seq...
In macromolecular X-ray crystallography, diffraction data sets are traditionally characterized by th...
A new probabilistic approach is introduced for the determination of the absolute structure of a comp...
The properties of synchrotron radiation relevant to single-crystal X-ray diffractometry are: its hig...
Owing to the two-dimensional periodicity of a super-structure on the crystal surface, the intensity ...
International audienceThe calibration of high-energy X-ray diffraction setups using an area detector...
Owing to the two-dimensional periodicity of a superstructure on the crystal surface, the intensity i...
This tutorial review article discusses chirality determination in the solid state, both in single cr...
The paper discusses several feasibility prediction criteria with particular emphasis on light atom m...
Single-crystal X-ray crystallography is the major analytical technique in use today for absolute-con...
Abstract. The first step in solving macromolecular crys-tal structures by multi- or single-wavelengt...
The paper describes measuring methods of weak resonant scattering signals occurring in X-ray diffrac...
It is shown that three-beam X-ray diffraction provides a means of resolving the enantiomorphism prob...
The phases of X-ray reflection of a crystal can be measured, except for an ambiguity, if the crystal...
Fundamental notions concerning absolute structure and absolute configuration, and their determinatio...
A Fortran program has been developed for the reduction of single-crystal diffraction data from a seq...
In macromolecular X-ray crystallography, diffraction data sets are traditionally characterized by th...
A new probabilistic approach is introduced for the determination of the absolute structure of a comp...
The properties of synchrotron radiation relevant to single-crystal X-ray diffractometry are: its hig...
Owing to the two-dimensional periodicity of a super-structure on the crystal surface, the intensity ...
International audienceThe calibration of high-energy X-ray diffraction setups using an area detector...
Owing to the two-dimensional periodicity of a superstructure on the crystal surface, the intensity i...
This tutorial review article discusses chirality determination in the solid state, both in single cr...