Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C37H36PBF4O3 CCI4

Frey, W.
Lieberknecht, A.
Griesser, H.
Bravo, Rodolfo Daniel
Colinas, Pedro Alfonso
Grigera, José Raúl

Publication date

June 2021

Journal

Zeitschrift für Kristallographie - New Crystal Structures

Abstract

Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.Centro de Estudios de Compuestos OrgánicosInstituto de Física de Líquidos y Sistemas Biológico

Extracted data

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Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>

Abstract

Extracted data

Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>

Abstract

Extracted data

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