The society is becoming increasingly more energy and environmentally conscientious, which has forced development of construction materials, which are both inexpensive and require very little energy to produce. One way of producing such materials is to utilize by-products of industrial processes. High-volume fly ash cement based grouts are tributary of such developements.This thesis outlines the results of a detailed study of the grain size distribution, three rheological properties and five mechanical properties of high-volume fly ash grouts (60% cement replacement for fly ash by weight) with or without the use of superplasticizers and/or anti-washout agents. The rheological properties are reported for eight water/cement + fly ash (water/so...