Measurement and Modelling of Soft Solid Layers in Cleaning Applications

Fouling and effective cleaning are important operating issues in the food and pharmaceutical industries, which need to be managed well to ensure process hygiene and productivity. In order to understand fouling and cleaning mechanisms, methods are required to quantify soft solid soil or deposit characteristics by measuring these in situ. This dissertation describes the development of millimanipulation and two new fluid dynamic gauging (FDG) devices, namely sideways FDG (SiDG) and integrated FDG (iFDG), and demonstrates their application for in situ measurement. Computational fluid dynamic (CFD) simulations of the flow patterns using the volume of fluid method were performed which enables previously inaccessible information to be extracted from the experimental data. The millimanipulation device reported by Magens et al., J Food Eng, 197 (2017) 48-59 measures the force experienced by a blade as it is pushed through a soil layer. The deformation of layers of viscoplastic petroleum jelly, soft white paraffin and toothpaste were studied and simulated using the regularized Bingham and the bi-viscosity models. The simulations gave good agreement with experimental results: combining visualisation and an interrupted testing mode allowed the material’s yield stress to be estimated. The SiDG device allows one to study the initial and long-term swelling of soft solid layers. The concept was implemented, commissioned and demonstrated by monitoring the swelling of gelatin, poly(vinyl acetate) (PVAc) and complex model soil layers at different pH and temperatures. All these materials underwent rapid initial hydration, followed by different longer term behaviour: gelatin and PVAc layers at pH < 11 exhibited Fickian diffusion control while at pH ≥ 11, PVAc exhibited relaxation control associated with hydrolysis. In the iFDG system the distances between the nozzle head and the soil layer, and the metallic substrate, are measured simultaneously by incorporating an inductive sensor in the gauging nozzle. The iFDG device was taken from concept to demonstration with a range of gauging liquids: water, UHT milk (opaque), a more viscous Newtonian fluid (washing-up liquid) and non-Newtonian aqueous solutions of 1 wt% and 3 wt% carboxymethyl cellulose (CMC). The CFD simulations gave good agreement with the experimental data. An ice growth experiment was performed using the iFDG device to demonstrate its application to monitoring growth of fouling layers. The CFD simulations were extended to consider the coupled flows which can arise in FDG measurements, where the stressed imposed by the gauging liquid flow can deform the soft solid soil layer. Two-fluid simulations were performed to estimate the change of topography of a petroleum jelly layer subject to FDG testing at different clearances. Acceptable agreement between the simulation results and measurements was obtained, and the observed differences were attributed to tubing-induced artefacts. A short feasibility study considered extending the approach to the three-fluid problem when a coherent liquid jet impinges horizontally on a horizontal plane coated with a soft solid soil layer. The results showed promising agreement with experiments on water jet cleaning of petroleum jelly layers.Taiwan Cambridge Scholarship (Cambridge Trust and Ministry of Education, Taiwan