Characterization and recyclability of 304L stainless steel powder for use in the selective laser melting process

Powder-bed fusion refers to a subset of additive manufacturing (AM) methods which successively melts and solidifies selected regions within a powder bed on a layer-by-layer basis to construct components directly from computer-aided design files. Laser Powder-Bed Fusion (L-PBF) is a process among the powder-bed fusion techniques that utilizes a laser to consolidate particles into a material with little porosity. During the L-PBF process, the large energy input from the laser causes the production of ejecta in the form of laser spatter and condensate, both of which have the potential to settle in the surrounding powder bed compromising its reusability. In order to better understand the impact of ejecta on powder recyclability, samples of 304L laser spatter and condensate were characterized in terms of morphology, chemistry, and microstructure. Differences between ejecta and virgin powder were used as a basis for understanding the evolution in 304L powder properties with reuse in the L-PBF process over the course of 7 iterations, which revealed an improvement in flowability with recycling. The effects of evolving powder properties on the tensile and impact toughness properties were also assessed for capturing possible deterioration in mechanical performance. Due to the improvement in powder flowability during recycling, the effects of alterations in the particle size were further investigated using the Discrete Element Method (DEM). Through development of a mathematical definition of spreadability, differences in the particle size distribution as well as recoating velocity and layer thickness revealed changes in the powder-bed quality providing crucial knowledge of the mechanisms behind the powder spreading process --Abstract, page iv