The objective of the study has been to verify the calculated residual activity in the decommissioning waste of the TRIGA Mark II–type research reactor FiR 1 in Finland. Knowledge of the radioactive inventory of irradiated materials is important in the planning of decommissioning activities and is essential for predicting the radiological impact to personnel and the environment. Measurements are performed for low active material samples from outer parts of the reactor. Methods include gamma spectrometric measurements, composition measurements with mass spectrometry, oxidation measurements of especially 14C in graphite, and full combustion measurements of lithium-enriched shielding materials. Results are compared to estimates calculated with ...