3-Bromo-1-(2,4-dichlorophenyl)-2-methoxy-3-(4-methoxyphenyl)propan-1-one–2-bromo-3-(3-chloro-4-methoxyphenyl)-1-(4-chlorophenyl)-3-methoxypropan-1-one (0.91/0.09)

Butcher, Ray J.
Jasinski, Jerry P.
Narayana, B.
Mayekar, Anil N.
Yathirajan, H. S.

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Publication date

October 2007

DOI

10.1107/S1600536807045977

Publisher

International Union of Crystallography (IUCr)

Abstract

The title co-crystal, 0.91C17H15BrCl2O3·0.09C17H15BrCl2O3, is a disordered mixture of two isomeric compounds. The ratio of the major and minor components in the co-crystal was obtained by refinement as 0.911 (3):0.089 (3). The dihedral angle between the two aromatic rings is 42.5 (2)°. Crystal packing is stabilized by intermolecular C—H⋯O hydrogen-bonding interactions which link the molecules into cyclic centrosymmetric R22(24) dimers

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3-Bromo-1-(2,4-dichlorophenyl)-2-methoxy-3-(4-methoxyphenyl)propan-1-one–2-bromo-3-(3-chloro-4-methoxyphenyl)-1-(4-chlorophenyl)-3-methoxypropan-1-one (0.91/0.09)

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3-Bromo-1-(2,4-dichlorophenyl)-2-methoxy-3-(4-methoxyphenyl)propan-1-one–2-bromo-3-(3-chloro-4-methoxyphenyl)-1-(4-chlorophenyl)-3-methoxypropan-1-one (0.91/0.09)

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3-Bromo-1-(2,4-di­chloro­phen­yl)-2-meth­­oxy-3-(4-meth­oxy­phen­yl)propan-1-one–2-bromo-3-(3-chloro-4-meth­oxy­phen­yl)-1-(4-chloro­phen­yl)-3-meth­oxy­propan-1-one (0.91/0.09)

Abstract

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3-Bromo-1-(2,4-di­chloro­phen­yl)-2-meth­­oxy-3-(4-meth­oxy­phen­yl)propan-1-one–2-bromo-3-(3-chloro-4-meth­oxy­phen­yl)-1-(4-chloro­phen­yl)-3-meth­oxy­propan-1-one (0.91/0.09)

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3-Bromo-1-(2,4-dichlorophenyl)-2-methoxy-3-(4-methoxyphenyl)propan-1-one–2-bromo-3-(3-chloro-4-methoxyphenyl)-1-(4-chlorophenyl)-3-methoxypropan-1-one (0.91/0.09)

3-Bromo-1-(2,4-dichlorophenyl)-2-methoxy-3-(4-methoxyphenyl)propan-1-one–2-bromo-3-(3-chloro-4-methoxyphenyl)-1-(4-chlorophenyl)-3-methoxypropan-1-one (0.91/0.09)