International audienceWe present an original experimental approach to the investigation of radiation-induced attenuation (RIA) mechanisms in optical fiber preforms. This protocol combines thermally stimulated luminescence (TSL) measurements with the characterization of RIA annealing during TSL readouts. It is systematically applied to compositions of increasing complexity to resolve the specific role played by each dopant. Silicate, aluminosilicate, Yb-doped silicate, Yb-doped and Yb,Ce-codoped aluminosilicate preform samples are examined. Annealing processes are described in detail as a function of temperature throughout TSL readouts. The protocol reveals the temperature ranges at which trapped-carrier states forming intrinsic or dopant-re...