CONTROLLED-POTENTIAL COULOMETRIC TITRATION OF URANIUM(VI) IN THE PRESENCE OF NITRATE

A study into the use of sulfamic acld as a nitritedestroying reagent in the controlled-potentlal coulometrlc tltratlon method for uranlum(VI) was made. When nltrites are thus destroyed, the tltration ls much less subject to error from HNO/sub 3/. The results of titratlons of known amounts of uranlum(VI) in the presence of varlous amounts of HNO/sub 3/, Th(NO/sub 3/)/sub 4/, Al(NO/sub 3/ )/sub 4/, and LiNO/sub 3/ are given. (auth