Use of Trispyrazolemethane in the Synthesis of Organometallic Compounds

  • Hazelton, Claire
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Publication date
January 2017
Publisher
Digital Commons @ Butler University
Language
English

Abstract

Trispyrazoleborate is a negatively charged facially coordinating tridentate ligand that has been highly researched and used in many metal complexes. The related ligand trispyrazolemethane has not been widely studied due to its difficult synthesis. The objective of this project is to determine the effects of the neutral nature of the trispyrazolemethane on the metal carbonyl complexes of molybdenum and tungsten. Besides the ligand tricarbonyl complex, iodide and hydride derivatives were synthesized. All compounds were characterized with IR and HNMR

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