Saturation Dislocation Microstructures In A Copper Single Crystal During Fatigue In HClO4 Aqueous Solution

ABSTRACT: A copper single crystal was tested at room temperature in air and in a 0.1M HClO4 solution under the symmetric tension-compression load mode, with loading axis parallel to the [013] direction. The dislocation structures were characterised using the electron channeling contrast (ECC) technique of scanning electron microscopy (SEM) and using transmission electron microscopy (TEM). The results show that the saturation dislocation structures in samples subjected to corrosion fatigue in the 0.1M HClO4 aqueous solution manly had the form of cells, dislocation wall-like and veins, which differ from the dislocation structures of dislocation wall-like and veins in the air environment.